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Home  >  Journal list  >  Journal of the Ceramic Society of Japan  >  Vol.117  No.1363 (March) (2009)  >  pp.356-358

Journal of the Ceramic Society of Japan
<<Previous article Vol.117  No.1363 (March) (2009)   pp.356 - 358 Next article>>

Preparation of layered double hydroxide coating films via the aqueous solution process using binary oxide gel films as precursor

Kiyofumi KATAGIRI1), Yurika GOTO1), Midori NOZAWA1) and Kunihito KOUMOTO1)
1) Department of Applied Chemistry, Graduate School of Engineering, Nagoya University

  Layered double hydroxides (LDHs) are inorganic materials consisting of the hydroxide layers formed with at least two metallic elements and anions between the layers. In this study, we have investigated the functionalization of LDH coating films by modification of both sol-gel and aqueous solution processes. A binary oxide system, Al2O3-TiO2, was used for the precursor gel films. Judging from XRD and SEM measurements, LDH crystals were generated for the wide range of gel composition. Therefore, coating films with composite structure of Zn-Al LDH and TiO2 was obtained by simple process. The reconstruction of LDH, i.e., heat treatment and following incubation in aqueous solution, was also achieved. This process can be expected for the intercalation of functional molecules in LDH layers and crystallization of TiO2 for these composite coatings.

Layered double hydroxide, Sol-gel method, Aqueous solution process, Crystal growth, Composite coating

Received: December 01, 2008
Accepted: January 15, 2009 , Published online: March 01, 2009
Copyright (c) 2009 The Ceramic Society of Japan



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