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Home  >  Journal list  >  Journal of the Ceramic Society of Japan  >  Vol.118  No.1381 (September) (2010)  >  pp.805-809

Journal of the Ceramic Society of Japan
<<Previous article Vol.118  No.1381 (September) (2010)   pp.805 - 809 Next article>>

Effect of CTAC concentration and Al precursor type on texture properties and microstructure of mesoporous alumina particles prepared by aerosol-assisted self-assembly

Joo Hyun KIM1), Kyeong Youl JUNG1) and Kyun Young PARK1)
1) Department of Chemical Engineering, Kongju National University

  The effect of the CTAC/Al ratio and the Al precursor type on the texture properties of alumina prepared by the evaporation-induced self-assembly (EISA) of aerosols was studied using N2 adsorption isotherms, small-angle X-ray scattering (SAXS), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). For the CTAC/Al ratio range 0.05 < CTAC/Al < 0.5 the prepared alumina particles had worm-like pore structure with a BET surface area of 170–365 m2/g and pore size of 2.7–3.4 nm. At CTAC/Al = 0.3, the largest surface area was achieved. The chloride precursor was most profitable to obtain the largest surface area (∼365 m2/g). However, the nitrate precursor was better for preparing non-hollow and mesoporous alumina, maintaining high surface area (∼320 m2/g) and pore regularity.


Keyword:
Mesoporous, Al2O3, Aerosol method, CTAC, Self assembly

Received: April 07, 2010
Accepted: July 15, 2010 , Published online: September 01, 2010
Copyright (c) 2010 The Ceramic Society of Japan

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